吴奕初
,
常香荣
,
田中卓
,
肖纪美
金属学报
本文采用正电子湮没技术研究了高纯Fe中的氢损伤规律,实验结果表明,在0.5mol/L H_2SO_4溶液中不加毒化剂电解充氢时,产生氢损伤的临界电流密度为20 mA/cm~2;而在0.5mol/L H_2SO_4溶液中加少量As_2O_3作为毒化剂电解充氢时,即使很小的电流密度也会产生氢损伤,配合慢拉伸试验,还发现试样内部产生氢损伤以后,它将控制随后的形变和断裂过程
关键词:
氢损伤
,
critical current density
,
positron annihilation technique
,
hydrogen-induced defect
郑亚萍
,
陈伟
,
李江红
,
许亚洪
复合材料学报
RTM和预浸料两种工艺共固化会形成一个界面层,采用差热分析和红外光谱研究环氧树脂/酸酐和环氧树脂/双氰胺共固化体系的反应,采用正电子湮没技术测试了共固化体系所形成界面中的自由体积尺寸和浓度.结果表明,单独体系的反应峰大约是1 60℃,两种工艺树脂混合后,反应峰向高温方向移动,为275.14℃；同时放热量从RTM体系的236.2 J/g和预浸料体系的193.9 J/g降低至83.15 J/g;界面层的自由体积尺寸和浓度比两个单独固化体系的大,弯曲强度分别从RTM体系的140.2 MPa和预浸科体系的105.4MPa降至83.4 MPa.两种体系的固化剂相互反应,致使共固化体系反应不完全,形成一个力学性能较低的共固化界面层.
关键词:
共固化
,
RTM工艺
,
预浸料
,
界面
,
正电子湮没技术
,
自由体积
WU Yichu CHANG Xiangrong TIAN Zhongzhuo XIAO Jimei University of Science and Technology Beijing
,
Beijing
,
China
金属学报(英文版)
Hydrogen damage in iron or 99.99% purity has been investigated by Doppler broadening measurement.Experimental results show that when the iron is charged with hydrogen in 0.5mol/L H_2SO_4 solution,the critical current density to cause hydrogen damage is 20mA/cm~2.While a little As_2O_3,saying 250mg/L,added to H_2SO_4 solution,even rather small current density.≤0.2mA/cm~2,would cause hydrogen damage.With the help ofi slow tensile test,it revealed that the hydrogen damage occurred in the specimen may be influential to the subsequent process of deformation and fracture.
关键词:
hydrogen damage
,
null
,
null
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